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| Title: | Total Synthesis of Rutaecarpine and Analogues by Tandem Azido Reductive Cyclization Assisted by Microwave Irradiation |
| Authors: | Kamal, A.
Reddy, M.K.
Reddy, T.S.
Santos, L.S.
Shankaraiah, N. |
| Keywords: | quinazolinones
beta-carbolines
azido-reductive cyclization
Ni2B
microwave irradiation |
| Issue Date: | 2011 |
| Publisher: | GEORG THIEME VERLAG |
| Citation: | SYNLETT Issue: 1 Pages: 61-64 DOI: 10.1055/s-0030-1259095 |
| Abstract: | The total synthesis of rutaecarpine and several analogues has been developed by using an azido reductive cyclization process starting from substituted azido benzoic acids. The intramolecular azido reductive cyclization step was performed with triphenylphosphine or Ni2B in HCl-MeOH (1 M) using microwave irradiation. This synthetic route is amenable for the generation of a library of quinazolinone compounds. |
| Description: | Santos, LS (Silva Santos, Leonardo). Univ Talca, Lab Asymmetr Synth, Chem Inst Nat Resources, Talca, Chile. |
| URI: | http://dspace.utalca.cl/handle/1950/9134 |
| ISSN: | 0936-5214 |
| Appears in Collections: | Artículos en publicaciones ISI - Universidad de Talca
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