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Please use this identifier to cite or link to this item: http://dspace.utalca.cl/handle/1950/9134

Title: Total Synthesis of Rutaecarpine and Analogues by Tandem Azido Reductive Cyclization Assisted by Microwave Irradiation
Authors: Kamal, A.
Reddy, M.K.
Reddy, T.S.
Santos, L.S.
Shankaraiah, N.
Keywords: quinazolinones
beta-carbolines
azido-reductive cyclization
Ni2B
microwave irradiation
Issue Date: 2011
Publisher: GEORG THIEME VERLAG
Citation: SYNLETT Issue: 1 Pages: 61-64 DOI: 10.1055/s-0030-1259095
Abstract: The total synthesis of rutaecarpine and several analogues has been developed by using an azido reductive cyclization process starting from substituted azido benzoic acids. The intramolecular azido reductive cyclization step was performed with triphenylphosphine or Ni2B in HCl-MeOH (1 M) using microwave irradiation. This synthetic route is amenable for the generation of a library of quinazolinone compounds.
Description: Santos, LS (Silva Santos, Leonardo). Univ Talca, Lab Asymmetr Synth, Chem Inst Nat Resources, Talca, Chile.
URI: http://dspace.utalca.cl/handle/1950/9134
ISSN: 0936-5214
Appears in Collections:Artículos en publicaciones ISI - Universidad de Talca

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